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Environmental testing and non-destructive failure analysis technology  
 
  Environmental testing and non-destructive failure analysis technology
  Shigeharu Yamamoto*
   This report will discuss failure analysis, and the methods of non-destructive failure analysis in particular, as used to improve quality by analyzing the occurrence of failures and providing feedback to the departments concerned. The report will also include some examples of testing and analysis.
 
1.Introduction
 
  Most manufacturers use environmental testing and failure analysis to maintain quality and reliability of products and parts.
  At the developmental stage, environmental testing is carried out to evaluate prototypes under conditions in which the product will be used, or according to test conditions determined by standards. In addition, when product failures occur in the marketplace, environmental testing is done to perform reproducible experiments as a part of failure analysis.
  When defects are reproduced through environmental testing, failure analysis is performed to clarify the cause of the failure and the results are provided as feedback to the design or manufacturing processes involved, and countermeasures are then taken. In this way, environmental testing and failure analysis are crucial measures for maintaining and improving product safety and reliability. This report will specifically focus on concrete instances of failure analysis in the first stage, in which non-destructive inspections are especially common. Fig.1 shows an outline of the product improvement process.
Fig. 1 Requirements for evaluation
  2.Approaches of failure analysis
(1) Even large systems are composed of units and individual subsystems, and those in turn are composed of individual parts, materials, and components that can be analyzed. Failures of these individual parts and materials cause an expanding ripple effect leading to failure of the entire system and causing major accidents. Because of this, reliability is maintained and safety is assured by specifying the causes of these failures and taking countermeasures.
(2) The bigger the system, the more crucial the problems posed by the interfaces between complex parts and units in which hard sections of individual parts and materials are combined with parts and materials of differing qualities. Accidents due to human contributions such as misuse and incorrect operation also form part of this equation. This can be well understood by looking at the recent Donen accident and airplane accidents.
(3) In general the cause of failure is said from experience to be due to:
1. Something that can be handled in design or at the design stage, 80%
2. Something caused in a production process, 15%
3. Something due to usage conditions, 5% Examples of matters that should be handled at the design stage include (a) constructions that lead to mistakes because the items is difficult to use, cannot be operated easily, or has complex operation, (b) constructions with difficult maintenance such as operations or processes that lead to incorrect operation. Problems at the design stage are more often due to insufficient design investigation (time/frequency, technology, properly qualified personnel) rather than the design itself.
(4) When failure is very slight, such as only one sample item or one set, product failure analysis looks at whether that failure is likely to have a major impact in the field. Waiting to see whether such failures occur in the field is thought to be too late, and so nowadays quality such as parts, materials, processes, and ease of operation are checked before shipping products to market. A number of examples are used to illustrate methods for looking in advance at the possibility of incorrect operation or failure, such as advance analysis (good product analysis) in addition to design investigation. One example is the pre-analysis of the inner conductivity conditions of multi-layer PCBs. (Refer to example 6-1.) Failure analysis considers potential and actual failure mechanisms and performs investigative research to provide corrective measures. These corrective measures can also be applied to other situations. When a failure occurs due to some cause, that cause can be identified as physical, chemical, mechanical, or electrical, or as due to human error. The results can always be explained in terms of the failure being caused according to a particular development.
  3.Methods of failure analysis
  Failure analysis can be broadly divided into de-structive and non-destructive testing. Potential defects and actual failures are identified and confirmed, and electrical, physical, chemical, and human engineering investigations are undertaken.
  These activities are crucial to creating countermeasures for the causes of failure. Fig. 2 shows the general procedure for failure analysis.


Fig. 2 Example of failure analysis
Two methods of locating failure are:
(1) The overall method {epidemiological method: non-destructive testing}, and
(2) The individual method {epidemiological method (physical failure method): destructive testing}.
  For procedure, less time is lost by taking up the epidemiological method first and the physical failure method later. An unexpectedly large number of failures can be found with the epidemiological method, but when the epidemiological and epidemiological methods are skillfully combined, reliability can be greatly improved.
(1) The epidemiological method
  This approach uses statistics to explain the degree of failure (e.g., according to time, place of occurrence, market distribution, market location, distribution of usage conditions, distribution of users, by lot, and time differences in manufacturing methods). Even if the reason for this type of failure is not understood, the range encompassing the failures can be narrowed down, and has the know-how to come up with effective countermeasures.
  This method can be used by anyone with no need for expensive equipment.
(2) The epidemiological method (physical failure method)
  This approach relies on completely grasping the mechanisms and principles of the failure and narrowing the actual cause to one point. In other words, this method has the know-how to theoretically understand why the failure occurred.
  Failure analysis clarifies the cause of failure, understands the failure mechanism, and links these to preventing recurrence of failure.
  In failure analysis, it is vital to obtain as much information as possible externally before making a destructive investigation, and normally non-destructive testing is done first. The extent of information obtained from this non-destructive testing will greatly influence later analysis and countermeasures.
  When performing failure analysis, the following specific items must be considered.
1) Don't analyze with insufficient investigation into factors such as shipping conditions, usage con-ditions, and usage environmental conditions.
2) Don't handle failure samples carelessly.
3) When investigating appearance, look at such conditions as dimensions, thickness, weight, shape, bending, color changes, rust, foreign matter adherence, mold, cracking, scratching, cloudiness, scorching, and nicking.
4) Since destructive analysis will cause the original shape and conditions to be lost, be sure to take plenty of pictures at the initial stage from every angle, of the piece as a whole, and with enlargements.
5) Carefully observe and record each time.
6) Since failure analysis uses tools and chemicals, consider worker safety.
7) Analyze failure objectively. Don't become convinced that a particular idea must be true.
8) Since the human factor is an important cause, consider the background carefully.
9) Analysis relies greatly on experience, skill, and power of observation.
10)  It is dangerous to ignore multiple causes and become convinced of a single cause.
11) Don't destroy the object by overloading.
12) Compare failed items with good items, and analyze the failures.
13) Consider effects from the workers themselves and from jigs, tools, and equipment used.
14) Don't throw away the specimens before final results have been attained. Keep them.
15) When making judgements, don't simply use the data alone as if it were analysis results.
16) Prepare good items from the same lot as the failed items. When the cause of failure is suspected to run across lots, good items must be investigated together across lots.
17) As a rule, proceed from the general situation to details to the overall picture. Also, go from external to internal analysis, from peripheral to the object, and from non-destructive to destructive.
18) Make full use of such elements as knowledge, ex-perience, and data. Ask for assistance from another specialist.
19) In failure analysis, when you have gone on to the next process, you can't go back, so you must observe very carefully at each stage of analysis.